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REFERENCE DOCUMENTS - RAL25/0004 (As Published)

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    Page                       : 9 of 11
    Work Order                 : ES2406465
    Client                     : ENVIRONMENTAL ADVISORS
    Project                    : 125 NSC LAKE McDONALD DVE, COOROY

    Sub-Matrix: SOIL                                                                                                       Method Blank (MB)                                Laboratory Control Spike (LCS) Report
                                                                                                                                Report                     Spike                  Spike Recovery (%)           Acceptable Limits (%)

     Method: Compound                                              CAS Number         LOR                   Unit                  Result              Concentration                      LCS                   Low              High

     EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 5634686) - continued
     EP231X: Perfluoroheptanoic acid (PFHpA)                        375-85-9         0.0002                mg/kg               <0.0002                0.00125 mg/kg                      102                  71.0               131
     EP231X: Perfluorooctanoic acid (PFOA)                          335-67-1         0.0002                mg/kg               <0.0002                0.00125 mg/kg                      101                  69.0               133

     EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 5634686)
     EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS)           757124-72-4         0.0005                mg/kg               <0.0005                0.00125 mg/kg                      79.0                 62.0               145
     EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS)            27619-97-2         0.0005                mg/kg               <0.0005                0.00125 mg/kg                      117                  64.0               140
     EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS)            39108-34-4         0.0005                mg/kg               <0.0005                0.00125 mg/kg                      102                  65.0               137
     EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS)         120226-60-0         0.0005                mg/kg               <0.0005                0.00125 mg/kg                      98.8                 69.2               143



    Matrix Spike (MS) Report
    The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on
    analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.
    Sub-Matrix: SOIL                                                                                                                                                               Matrix Spike (MS) Report

                                                                                                                                                                        Spike          SpikeRecovery(%)       Acceptable Limits (%)
     Laboratory sample ID   Sample ID                                             Method: Compound                                             CAS Number          Concentration                MS             Low              High

     EG005(ED093)T: Total Metals by ICP-AES (QCLot: 5633361)
      ES2404940-001         Anonymous                                             EG005T: Arsenic                                              7440-38-2              50 mg/kg                 97.2           70.0             130
                                                                                  EG005T: Cadmium                                              7440-43-9              50 mg/kg                 92.8           70.0             130
                                                                                  EG005T: Chromium                                             7440-47-3              50 mg/kg                  102           68.0             132
                                                                                  EG005T: Copper                                               7440-50-8            250 mg/kg                  88.9           70.0             130
                                                                                  EG005T: Lead                                                 7439-92-1            250 mg/kg                  93.6           70.0             130
                                                                                  EG005T: Nickel                                               7440-02-0              50 mg/kg                 93.6           70.0             130
                                                                                  EG005T: Zinc                                                 7440-66-6            250 mg/kg                  75.0           66.0             133

     EG035T: Total Recoverable Mercury by FIMS (QCLot: 5633362)
      ES2404940-001         Anonymous                                             EG035T: Mercury                                              7439-97-6              5 mg/kg                  79.7           70.0             130

     EP066: Polychlorinated Biphenyls (PCB) (QCLot: 5630465)
      ES2406444-001         Anonymous                                             EP066: Total Polychlorinated biphenyls                       ----                   1 mg/kg                  98.0           70.0             130
     EP068A: Organochlorine Pesticides (OC) (QCLot: 5630464)
      ES2406444-001         Anonymous                                             EP068: gamma-BHC                                             58-89-9                0.5 mg/kg                79.1           70.0             130
                                                                                  EP068: Heptachlor                                            76-44-8                0.5 mg/kg                93.2           70.0             130
                                                                                  EP068: Aldrin                                                309-00-2               0.5 mg/kg                85.5           70.0             130
                                                                                  EP068: Dieldrin                                              60-57-1                0.5 mg/kg                87.2           70.0             130
                                                                                  EP068: Endrin                                                72-20-8                2 mg/kg                  78.0           70.0             130
                                                                                  EP068: 4.4`-DDT                                              50-29-3                2 mg/kg                  86.0           70.0             130

     EP068B: Organophosphorus Pesticides (OP) (QCLot: 5630464)
      ES2406444-001         Anonymous                                             EP068: Diazinon                                              333-41-5               0.5 mg/kg                76.1           70.0             130

Document Set ID: 23717062
Version: 0, Version Date: 01/01/1900

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