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REFERENCE DOCUMENTS - RAL25/0004 (As Published)
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Page : 2 of 4
Work Order : EB2307800
Client : ENVIRONMENTAL ADVISORS
Project : 125 NSC LAKE McDONALD DVE, COOROY
General Comments
The analytical procedures used by ALS have been developed from established internationally recognised procedures such as those published by the USEPA, APHA, AS and NEPM. In house developed procedures
are fully validated and are often at the client request.
Where moisture determination has been performed, results are reported on a dry weight basis.
Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract /digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from
standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.
Key : Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot
CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.
LOR = Limit of reporting
RPD = Relative Percentage Difference
# = Indicates failed QC
Laboratory Duplicate (DUP) Report
The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges
for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:
No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Laboratory sample ID Sample ID Method: Compound CAS Number LOR Unit Original Result Duplicate Result RPD (%) Acceptable RPD (%)
EG005(ED093)T: Total Metals by ICP-AES (QC Lot: 4934343)
EB2307649-001 Anonymous EG005T: Chromium 7440-47-3 2 mg/kg 19 9 68.4 No Limit
EA055: Moisture Content (Dried @ 105-110°C) (QC Lot: 4934346)
EB2307649-001 Anonymous EA055: Moisture Content ---- 0.1 % 8.4 8.6 2.6 0% - 20%
EG048: Hexavalent Chromium (Alkaline Digest) (QC Lot: 4934344)
EB2307718-001 Anonymous EG048G: Hexavalent Chromium 18540-29-9 0.5 mg/kg <39.1 <39.7 1.6 No Limit
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Laboratory sample ID Sample ID Method: Compound CAS Number LOR Unit Original Result Duplicate Result RPD (%) Acceptable RPD (%)
EG005(ED093)C: Leachable Metals by ICPAES (QC Lot: 4943154)
EB2307800-001 TP9-0.1 EG005C: Cadmium 7440-43-9 0.05 mg/L <0.05 <0.05 0.0 No Limit
EG005C: Arsenic 7440-38-2 0.1 mg/L <0.1 <0.1 0.0 No Limit
EG005C: Chromium 7440-47-3 0.1 mg/L <0.1 <0.1 0.0 No Limit
EG005C: Copper 7440-50-8 0.1 mg/L <0.1 <0.1 0.0 No Limit
EG005C: Lead 7439-92-1 0.1 mg/L 0.6 0.6 0.0 No Limit
EG005C: Nickel 7440-02-0 0.1 mg/L <0.1 <0.1 0.0 No Limit
EG005C: Zinc 7440-66-6 0.1 mg/L 4.4 4.4 0.0 0% - 20%
EG035C: Leachable Mercury by FIMS (QC Lot: 4941920)
EB2307421-001 Anonymous EG035C: Mercury 7439-97-6 0.0001 mg/L <0.0010 <0.0010 0.0 No Limit
EB2308080-002 Anonymous EG035C: Mercury 7439-97-6 0.0001 mg/L 0.0036 0.0037 3.3 No Limit
Document Set ID: 23717062
Version: 0, Version Date: 01/01/1900
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